Yes, I mixed it in room temperature bottled still water. I guess I added it about a minute or so after I diluted it in the water, perhaps more. After diluting it, what's the longest you can wait before adding it? After two hours of nothing setting, I added a few more drops directly to the milk (figured there's nothing to lose). Waited another hour, nothing. Still looks just like milk. In the end, supposing the rennet is dud, I heated the milk up to 185F and added some vinegar and lemon, as I've done in the past, to make an easy queso blanco kind of thing. That usually sets it within a few minutes. Again nothing - although obviously I have no idea how dud rennet (if that's what it is) might have affected the ability of milk to curdle.